Analytical Profiles of Drug Substances, Vol. 1 by FLOREY KLAUS PDF

By FLOREY KLAUS

ISBN-10: 0122608011

ISBN-13: 9780122608018

Profiles of Drug ingredients, Excipients and similar method vol 1. content material: entrance conceal; Analytical Profiles of Drug ingredients, quantity 1; Copyright web page; Contents; AFFILIATIONS OF EDITORS, individuals, AND REVIEWERS; FOREWORD; PREFACE; bankruptcy 1. Acetohexamide; bankruptcy 2. Chlordiazepoxide; bankruptcy three. Chlordiazepoxide Hydrochloride; bankruptcy four. Cycloserine; bankruptcy five. Cyclothiazide; bankruptcy 6. Diazepam; bankruptcy 7. Erythromycin Estolate; bankruptcy eight. Halothane; bankruptcy nine. Levarterenol Bitartrate; bankruptcy 10. Meperidine Hydrochloride; bankruptcy eleven. Meprobamate; bankruptcy 12. Nortriptyline Hydrochloride; bankruptcy thirteen. Potassium Phenoxymethyl Penicillin. bankruptcy 14. Propoxyphene HydrochlorideChapter 15. Sodium Cephalothin; bankruptcy sixteen. Sodium Secobarbital; bankruptcy 17. Triamcinolone; bankruptcy 18. Triamcinolone Acetonide; bankruptcy 19. Triamcinolone Diacetate; bankruptcy 20. Vinblastine Sulfate; bankruptcy 21. Vincristine Sulfate. summary: Profiles of Drug elements, Excipients and comparable method vol 1

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6 M e l t i n g Range C h l o r d i a z e p o x i d e melts w i t h decomposition. The range d e s c r i b e d i n USP X V I I I i s 212-218OC u s i n g Class I method 7. 7 D i f f e r e n t i a l Scanning C a l o r i m e t r y The DSC s p e c t r u m of c h l o r d i a z e p o x i d e h y d r o c h l o r i d e is shown i n F i g u r e 3. The exotherm observed a t 233°C c o r r e s p o n d s t o t h e m e l t i n g of t h e d r u g f o l l o w e d by decomp o s i t i o n a t a p p r o x i m a t e l y 241OC.

Lting endot h e r m , f o l l o w e d by a r a p i d e x o t h e r m was o b servedo A t a h e a t i n g r a t e o f 20 C/min. the endotherm peaked a t 152 C and t h e exotherm a t 150 C. 0;6 w e i g h t l o s s a t 1 4 7 C. Lieight l o s s o c c u r r e d r a p i d l y a s t h e t e m p e r a t u r e approached the melting (decomposition) p o i n t , The m e a s u r e m e n t was p e r f o r m e d u n d e r n i t r o g e n 57 J. W. LAME sweep a t a h e a t i n g G a t e o f 5 C/min. 8 Solubility T h e f o l l o w i n g s o l u b i l i t y d a t a were Cycloserine is esseno b t a i n e d f r o m Ir'eiss6.

4 2000 c/S f u l l s c a l e Chart speed 1 inch p e r 5 minutes 25 A. MacDONALD, A. F. MICHAELIS, AND 6. 2 . SENKOWSKI Samples p r e p a r e d by g r i n d i n g a t room t e m p e r a t u r e . 12 Distribution Coefficient Reymond and Toome1*=d t h e d i s t r i b u t i o n coe f f i c i e n t of c h l o r d i a z e p o x i d e between n - o c t a n o l and pH 7 . 2 b u f f e r t o have a v a l u e o f l 7 l a t room t e m p e r a t u r e where D = Coctanol/Cbuffer12. 26 CH LORD1AZEPOXI DE 3. Synthesis Chlordiazepoxide is prepared by the reaction scheme shown in Figure 6 .

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Analytical Profiles of Drug Substances, Vol. 1 by FLOREY KLAUS


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